https://eln.excellgen.com/index.php?action=history&feed=atom&title=Synthesis_of_1%2C3-Dibromo-2-propanol 2026-10-18T08:18:39Z Revision history for this page on the wiki MediaWiki 1.44.0 https://eln.excellgen.com/index.php?title=Synthesis_of_1,3-Dibromo-2-propanol&diff=12422&oldid=prev 2014-07-15T02:45:51Z

<p>Created page with &quot;Amorphous phosphorus (6.5 g) and glycerol&lt;br&gt;(28.0 g) were added into the 250ml round bottom flask. The mixture was stirred by mechanical&lt;br&gt;force. The bromine (52.8 g) was then ...&quot;</p> <p><b>New page</b></p><div>Amorphous phosphorus (6.5 g) and glycerol&lt;br&gt;(28.0 g) were added into the 250ml round bottom flask. The mixture was stirred by mechanical&lt;br&gt;force. The bromine (52.8 g) was then slowly added with a temperature less than 80°C. This&lt;br&gt;process took about 2 h and stirring was continued for another 2 h .Then the mixture was kept&lt;br&gt;overnight. The saturated solution of sodium sulfite was added into the mixture to remove the&lt;br&gt;residue bromine. The crude product was washed with saturated solution of sodium chloride three&lt;br&gt;times and dried by anhydrous sodium sulfate. After vacuum distillation, 1, 3- dibromo-2-propanol&lt;br&gt;was obtained as transparent and colorless liquid with the yield of 61.3%.&lt;br&gt;<br /> <br /> [[Category:Transfection]][[Category:Paul]]</div>

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